含三氟甲硫基/二氟甲硫基试剂的创制及其反应性能研究

21572258
2015
B0101.元素化学
沈其龙
面上项目
研究员
中国科学院上海有机化学研究所
75万元
亲电取代;三氟甲硫基;手性含氟化合物;氟烷基;二氟甲硫基
2016-01-01到2019-12-31
  • 中英文摘要
  • 结题摘要
  • 结题报告
  • 项目成果
  • 项目参与人
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序号 标题 类型 作者
1 二氟甲基取代的硫代芳基磺酸酯、其制备方法及应用 专利 沈其龙;吕龙;朱佃虎;邵欣欣
2 A Two-Step, One-Pot, and Multigram-Scale Synthesis of N-Difluoromethylthiophthalimide 期刊论文 Zhu Dianhu;Hong Xin;Li Dezhi;Lu Long;Shen Qilong
3 Direct Monofluoromethylthiolation with S-(Fluoromethyl) Benzenesulfonothioate 期刊论文 Zhao Qunchao;Lu Long;Shen Qilong
4 三氟甲硫基化试剂、合成方法及其应用 专利 沈其龙;徐春发
5 N-Trifluoromethylthio-dibenzenesulfonimide: A Shelf-Stable, Broadly Applicable Electrophilic Trifluoromethylthiolating Reagent 期刊论文 Zhang Panpan;Li Man;Xue Xiao-Song;Xu Chunfa;Zhao Qunchao;Liu Yafei;Wang Haoyang;Guo Yinlong;Lu Long;Shen Qilong
6 三氟甲基硫代过氧化物及其制备方法 专利 沈其龙;徐春发
7 Synthesis and Reactivity of a-Cumyl Bromodifluoromethanesulfenate: Application to the Radiosynthesis of [18F]ArylSCF3 期刊论文 Jiang Wu;Qunchao Zhao;Thomas C. Wilson;Stefan Verhoog;Long Lu;Veronique Gouverneur;Qilong Shen
8 含三氟甲硫基的化合物及其制备方法 专利 沈其龙;徐春发
9 PhSO2SCF2H: A Shelf-Stable, Easily Scalable Reagent for Radical Difluoromethylthiolation 期刊论文 Zhu Dianhu;Shao Xinxin;Hong Xin;Lu Long;Shen Qilong
10 (1S)-(−)-N-Trifluoromethylthio-2,10- camphorsultam and its derivatives: easily available, optically pure reagents for asymmetric trifluoromethylthiolation 期刊论文 He Zhang;Xuebing Leng;Xiaolong Wan;Qilong Shen
11 Copper-Catalyzed Carbene Insertion into the Sulfur–Sulfur Bond of RS–SCF2H/SCF3 under Mild Conditions 期刊论文 Xin Hong;Long Lu;Qilong Shen
12 Radical fluoroalkylthiolation of aldehydes with PhSO2SRf (Rf = CF3, C2F5, CF2H or CH2F): a general protocol for the preparation of fluoroalkylthioesters 期刊论文 Bin Xu;Dezhi Li;Long Lu;Decai Wang;Yonghong Hu;Qilong Shen
13 Transition-Metal-Free ipso-Trifluoromethylthiolation of Lithium Aryl Boronates 期刊论文 Feng Shen;Hanliang Zheng;Xiao-Song Xue;Long Lu;Qilong Shen
14 Pd Catalyzed Difluoromethylthiolation of Aryl Chlorides Bromides and Triflates 期刊论文 Jiang Wu;Changhui Lu;Long Lu;Qilong Shen
15 Asymmetric Difluoromethylthiolation of Carbon Nucleophiles with Optically Pure Difluoromethylthiolating Reagents Derived from Camphorsultam 期刊论文 Zhang He;Wan Xiaolong;Shen Qilong
16 Silver-catalyzed ring-opening difluoromethylthiolation/trifluoromethylthiolation of cycloalkanols with PhSO2SCF2H or PhSO2SCF3 期刊论文 Bin Xu;Decai Wang;Yonghong Hu;Qilong Shen
17 [[(Ethoxycarbonyl)difluoromethyl]thio]phthalimide: A Shelf-Stable, Electrophilic Reagent with a Convertible Group for the Synthesis of Diversified Fluoroalkylthiolated Compounds 期刊论文 Feng Shen;Panpan Zhang;Long Lu;Qilong Shen
18 Cobalt-catalyzed hydro-difluoromethylthiolation/hydrotrifluoromethylthiolation of unactivated alkenes 期刊论文 Xinxin Shao;Xin Hong;Long Lu;Qilong Shen
19 Palladium-catalyzed difluoromethylthiolation of heteroaryl bromides, iodides, triflates and aryl iodides 期刊论文 Wu Jiang;Liu Yafei;Lu Changhui;Shen Qilong
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