基于三元杂环与卡宾和乃春的杂环化合物合成

21572017
2015
B0108.新反应与新试剂
许家喜
面上项目
教授
北京化工大学
65万元
三元杂环;卡宾;叶立德;扩环反应;乃春
2016-01-01到2019-12-31
  • 中英文摘要
  • 结题摘要
  • 结题报告
  • 项目成果
  • 项目参与人
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序号 标题 类型 作者
1 Oxygenophilic Lewis acid-promoted synthesis of 2-arylindoles from anilines and cyanoepoxides in alcohol. 期刊论文 Xu， Chuangchuang;Xu Jiaxi
2 一种苯并[b][1,4]氧硫杂环己3基甲醇的制备方法 专利 许家喜;董军
3 Selectivities in the Microwave-Assisted Organic Reactions 专著 Jiaxi Xu
4 Sulfur-directed metal-free and regiospecific methyl C(sp(3))-H imidation of thioanisoles 期刊论文 Yang Zhanhui;Yang Shiyi;Xu Jiaxi
5 Specific intramolecular aromatic C-H insertion of diazosulfonamides 期刊论文 Huang Peipei;Yang Zhanhui;Xu Jiaxi
6 Safe, Metal-Free, and Direct Synthesis of Dialkyl Acylmethylidenehydrazine-1,1-dicarboxylates from Dimethylsulfoxonium Acylmethylides and Dialkyl Azodicarboxylates 期刊论文 Zhou Bingnan;Dong Jun;Xu Jiaxi
7 A concise synthesis of cyclobrassinin and its analogues via a thiyl radical aromatic substitution 期刊论文 Zhong Xin;Chen Ning;Xu Jiaxi
8 Retro-Corey-Chaykovsky Epoxidation: Converting Geminal Disubstituted Epoxides to Ketones 期刊论文 Li Siqi;Li Pingfan;Xu Jiaxi
9 Microwave-assisted copper-catalyzed stereoselective ring expansion of three-membered heterocycles with alpha-diazo-beta-dicarbonyl compounds 期刊论文 Siqi Li;Xingpeng Chen;Jiaxi Xu
10 Na2S2O8-mediated efficient synthesis of isothiocyanates from primary amines in water 期刊论文 Fu Zhicheng;Yuan Wenhao;Chen Ning;Yang Zhanhui;Xu Jiaxi
11 Microwave-assisted organic acid-base-co-catalyzed tandem Meinwald rearrangement and annulation of styrylepoxides. 期刊论文 Shi Yi;Li Siqi;Lu Yang;Zhao Zizhen;Li Pingfan;Xu Jiaxi
12 Metal-free and regiospecific synthesis of 3-arylindoles. 期刊论文 Xu Chuangchuang;Xie Wenlai;Xu Jiaxi
13 Stereochemistry and Mechanistic Insight in the [2(k)+2(i)+2(i)] Annulations of Ketenes and Imines 期刊论文 Yang Zhanhui;He Wei;Cheng Baoxiang;Xu Jiaxi
14 铜催化的硫叶立德和偶氮二甲酸酯的反应 期刊论文 周柄男;董军;许家喜
15 氮杂环丁烷的合成 期刊论文 符志成;许家喜
16 Synthesis of Sulfonylhydrazine-1,2-dicarboxylates from Thiols and Dialkyl Azodicarboxylates 期刊论文 Zhou Bingnan;Yang Xiao;Xu Jiaxi
17 Synthesis of 2-oxophosphorindolines via the copper-catalyzed intramolecular aromatic C-H insertion of diazophosphonamidates 期刊论文 Huang Peipei;Xu Jiaxi
18 Sulfur-mediated C(sp(2))-H imidation and 1,2-imidofluorination of vinyl sulfides 期刊论文 Yang Zhanhui;Yang Shiyi;Haroone Muhammad Sohail;He Wei;Xu Jiaxi
19 Improved Buchner reaction selectivity in the copper-catalyzed reactions of ethyl 3-arylmethylamino-2-diazo-3-oxopropanoates 期刊论文 Jing Liu;Jianzhuo Tu;Zhanhui Yang;Chol-Ung Pak;Jiaxi Xu
20 Temperature-dependent annuloselectivity and stereochemistry in the reactions of methanesulfonyl sulfene with imines 期刊论文 Wu Qiuyue;Yang Zhanhui;Xu Jiaxi
21 Facile synthesis of thietanes via ring expansion of thiiranes 期刊论文 Dong Jun;Xu Jiaxi
22 氨基甲酸酯在C—H键活化中的应用 期刊论文 阙楚强;陈宁;许家喜
23 Sulfur-Mediated Electrophilic Cyclization of Aryl-Substituted Internal Alkynes 期刊论文 Zhang Zhong;He Pan;Du Hongguang;Xu Jiaxi;Li Pingfan
24 (N-芳基亚磺酰基)磺酰肼及其制备方法 专利 许家喜;杨占会
25 Nucleophilic Organic Base DABCO-Mediated Chemospecific Meinwald Rearrangement of Terminal Epoxides into Methyl Ketones 期刊论文 Li Siqi;Shi Yi;Li Pingfan;Xu Jiaxi
26 Chiral synthesis of McGeachin-type bisaminals. 期刊论文 Chen Yang;Li Siqi;Hou Shili;Xu Jiaxi;Yang Zhanhui
27 Regiospecific synthesis of polysubstituted furans with mono- to tricarboxylates from various sulfonium acylmethylides and acetylenic esters 期刊论文 Dong Jun;Du Hongguang;Xu Jiaxi
28 An expeditious method to synthesize difluoroboron complexes of beta-keto amides from beta-keto nitriles and BF3 center dot OEt2 期刊论文 Xu Chuangchuang;Xu Jiaxi
29 Efficient synthesis of N-benzyloxycarbonyl-2-aminoalkanesulfonyl chlorides with functionalized side-chains. 期刊论文 Abdellaoui Hassane;Chen Xingpeng;Xu Jiaxi
30 BF3·OEt2-promoted tandem Meinwald rearrangement and nucleophilic substitution of oxiranecarbonitriles 期刊论文 Xu Chuangchuang;Xu Jiaxi
31 Expeditious and Convenient Synthesis of Polycyclic Difluoroboron Complexes of 2-Oxoindoline-3-carboxamides by Tandem Reaction 期刊论文 Mo Shanyan;Xu Chuangchuang;Xu Jiaxi
32 Aminoxidation of Arenethiols to N-Chloro-N-sulfonyl Sulfinamides 期刊论文 Yang Zhanhui;Xu Wei;Wu Quyue;Xu Jiaxi
33 Thermal conversion of primary alcohols to disulfides via xanthate intermediates: an extension to the Chugaev elimination 期刊论文 He Wei;Ding Yong;Tu Jianzhuo;Que Chuqiang;Yang Zhanhui;Xu Jiaxi
34 Cobalt-Catalyzed Cycloisomerization of N,N-Diallylanilines 期刊论文 Liu Jun;Yang Zhanhui;Zheng Minfang;Wu Hongfei;Chen Ning;Xu Jiaxi
35 Transition metal-free access to 3,4-dihydro-1,2-oxaphosphinine-2-oxides from phosphonochloridates and chalcones through tandem Michael addition and nucleophilic substitution 期刊论文 Fu Zhicheng;Sun Simin;Yang Anjian;Sun Fang;Xu Jiaxi
36 Iridium-catalyzed efficient reduction of ketones in water with formic acid as a hydride donor at low catalyst loading 期刊论文 Liu Ji-tian;Yang Shiyi;Yang Zhanhui;Tang Weiping;Xu Jiaxi
37 Safe and Metal-Free Synthesis of 1-Alkenyl Aryl Sulfides and Their Sulfones from Thiiranes and Diaryliodonium Salts 期刊论文 Dong Jun;Xu Jiaxi
38 Microwave-Assisted CuCl-Catalyzed Three-Component Reactions of Alkynes, Aldehydes, and Amino Alcohols 期刊论文 Li Xiang;Chen Ning;Xu Jiaxi
39 Theoretical calculation studies on the rearrangement mechansims of arenesulfenanilides to o- and p-aminodiphenyl sulfides. 期刊论文 Liu Guangyan;Hou Shili;Xu Jiaxi
40 Synthesis of N-alkylated 2-pyridones through Pummerer type reactions of activated sulfoxides and 2-fluoropyridine derivatives 期刊论文 Hu Gang;Xu Jiaxi;Li Pingfan
41 Sulfur mediated propargylic C-H alkylation of alkynes 期刊论文 Hu Gang;Xu Jiaxi;Li Pingfan
42 一种3酰基1,4氧硫杂环己烯的制备方法 专利 许家喜;陈兴鹏
43 Methanesulfinylation of benzyl halides with dimethyl sulfoxide. 期刊论文 Fu Duo;Dong Jun;Du Hongguang;Xu Jiaxi
44 Tertiary amine-catalyzed and direct synthesis of alpha-chloroalkanesulfonythydrazines from azodicarboxylates and sulfonyl chlorides 期刊论文 Zhou Bingnan;Xu Jiaxi
45 Intramolecular Carbene C-H Insertion Reactions of 2-Diazo-2-sulfamoylacetamides 期刊论文 Que Chuqiang;Huang Peipei;Yang Zhanhui;Chen Ning;Xu Jiaxi
46 Mechanistic insight into the thermal 1,3-chlorine migrations of N-chloroacetanilides under neutral conditions 期刊论文 Cheng Baoxiang;Xu Jiaxi
47 NBS/DMSO-mediated synthesis of (2,3-dihydrobenzo[b][1,4]oxathiin-3-yl)methanols from aryloxymethylthiiranes 期刊论文 Dong Jun;Xu Jiaxi
48 Chemospecific synthesis of 2-acetoxyindole-3-carbonitriles catalyzed by Cu(acac)(2) 期刊论文 Mo Shanyan;Tu Jianzhuo;Xu Jiaxi
49 Synthesis of alpha-heterosubstituted ketones through sulfur mediated difunctionalization of internal alkynes 期刊论文 Zhang Zhong;Luo Yuzheng;Du Hongguang;Xu Jiaxi;Li Pingfan
50 A Tandem Sulfonylation and Knoevenagel Condensation for the Preparation of Sulfocoumarin-3-carboxylates 期刊论文 Dong Ziyang;Chen Yang;Yang Zhiheng;Yang Zhanhui;Xu Jiaxi
51 Synthesis of Functionalized Thietanes via Electrophilic Carbenoid-Induced Ring Expansion of Thiiranes with Sulfonium Acylmethylides as Carbene Precursors 期刊论文 Dong Jun;Du Hongguang;Xu Jiaxi
52 BF3·OEt2-Catalyzed synthesis of anti-β-(N-arylamino)-α-hydroxynitriles by regio- and diastereospecific ring-opening of 3-aryloxirane-2-carbonitriles with anilines. 期刊论文 Xu Chuangchuang;Lu Yang;Xu Kaini;Xu Jiaxi
53 Synthesis of Four- to Seven-Membered Heterocycles by Ring Expansion: Ring Expansions of Thiiranes and Thietanes 专著 Jiaxi
54 Efficient Direct Synthesis of Aziridine-Containing Chiral Tridentate Ligands by the Iminium-Mediated Self-Ring Opening Reaction of Enantiopure Aziridines and Salicylaldehydes 期刊论文 Chen Xingpeng;Lin Chao;Du Hongguang;Xu Jiaxi
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